Thor, Vol. 1 #242 (1975)

When the Servitor Commands!
Thor, Odin, and Jane leave the pyramid, and Thor uses Mjolnir to send it elsewhere. With the pyramid gone, Odin's full memory returns. Odin is furious that Thor is still with Jane Foster, and he is not welcome in Asgard until he has forsworn her forever. Thor flies Jane back to her apartment, where they find the Warriors Three. Before long, a gigantic hand crashes through the wall and grabs Jane. The four warriors defeat the Servitor, but before Thor can finish him off, he is stopped by Zarrko - who needs Thor's help.
Release Date: 1975