Ultimate Spider-Man, Vol. 1 #26 (2002)

Circles
Mary Jane wakes up, and Peter sends her to safety in a cab. As soon as the pair are clear of Osborn, S.H.I.E.L.D. opens fire, driving him away from the scene. Peter follows him back to his home, where Norman takes another shot of Oz and beats Peter badly, just before Harry wakes up to witness events unfolding.
Release Date: 2002