Captain America, Vol. 5 #32 (2007)

The Burden of Dreams, Part Two: The Death of Captain America, Act 2
The Winter Soldier has managed to resist Dr. Faustus' attempts to place him under the control of the Red Skull thus far, but Faustus is only getting started. But an attack on his lair by the Falcon and the Black Widow forces Faustus to evacuate. But in the chaos of the evacuation, Agent 13 attempts to fight Faustus' conditioning. Can she get free of it in time to save the Winter Soldier's life?
Release Date: 2007