Ultimate Spider-Man, Vol. 1 #77 (2005)

Hobgoblin, Part 6
Peter is trying to subdue Harry without seriously harming him, but they've drawn the attention of S.H.I.E.L.D., who are not similarly restrained. Peter vents his frustration at Nick Fury, who says much more after Peter leaves than when Peter was there. Peter returns home to find Mary Jane, and they have a meaningful discussion of their own.
Release Date: 2005