Ultimate Spider-Man, Vol. 1 #115 (2007)

Death of A Goblin, Part 4
Peter wakes up in a S.H.I.E.L.D. holding cell, where he and Captain Carol Danvers have a good heart-to-heart talk, until Kitty shows up to rescue him. On the way out, they learn Danvers' true motives; she publically captured Spider-Man, hoping Norman Osborn would come to S.H.I.E.L.D. to get him. Instead, Norman's been looking for the men who stole his money, and Danvers recruits Spider-Man and Shadowcat to help take him down.
Release Date: 2007